01
Reaction #1198758
Reaction scheme
No renderable structure data available
No renderable structure data available
No renderable structure data available
No renderable structure data available
No renderable structure data available
No renderable structure data available
Related Literature (1)
openreactiondata ↗doi:10.6084/m9.figshare.5104873.v1; patent:US07615661B2
Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: Ethyl 2-bromoisobutyrate (48.8 g, 0.250 mole), sodium hydrosulfide hydrate (84 g, 1.5 mole), water (100 mL), ethyl alcohol (200 mL). Let reaction mix stir at room temperature. Next day, no starting material observed. Crude yield: 74.3%; distillation yield: 36.0%. reaction mix distillation yield: 36.0%
Source ID: ord-e75733b00fb949a88f3a90873c089504