No renderable structure data available
C1=CC(=C(C(=C1)O)C(=O)N)OChemical Intermediate
Structures, identifiers and computed properties have been matched to the database record by CAS.
| Intermediates | 2,6-dihydroxybenzamide |
|---|---|
| IUPAC Name | — |
| CAS Number | 3147-50-0 |
| Database ID | 76602 |
| Molecular Formula | — |
| Molecular Weight | — |
Product Information
2,6-dihydroxybenzamide (CAS 3147-50-0) product identity, structure identifiers and related reaction data for chemical intermediate research and sourcing review.
Potential Applications
For professional research and industrial use only
Database ID 76602
Safety Notice
For professional research and industrial use only. Review the supplier safety data sheet before handling.
Synthesis data
12 reactions · 12 references
Conditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-96793f9fcc584dfda0813e03b1c3d606Conditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-77dca147f7b040fa94903350b02c0755Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: A mixture of 23.0 g of 2,6-dihydroxybenzamide, 20.7 g of potassium carbonate and 28.2 g of 1,2-dibromoethane is refluxed, whilst stirring, for 2-3 hours in 300 ml of acetonitrile. The reaction mixture is filtered whilst still warm, the filtrate concentrated by evaporation and the residue recrystallised from a little methanol. 6-(2-Bromoethoxy)salicylamide having a melting point of 120°-121° is obtained. is refluxed The reaction mixture is filtered whilst still warm the filtrate concentrated by evaporation the residue recrystallised from a little methanol
Source ID: ord-6f3ffc5c3dae437286a22103a3ef822fConditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: A mixture of 23.0 g of 2,6-dihydroxybenzamide, 20.7 g of potassium carbonate and 28.2 g of 1,2-dibromoethane is refluxed, whilst stirring, for 2-3 hours in 300 ml of acetonitrile. The reaction mixture is filtered whilst still warm, the filtrate concentrated by evaporation and the residue recrystallised from a little methanol. 6-(2-Bromoethoxy)salicylamide having a melting point of 120°-121° is obtained. is refluxed The reaction mixture is filtered whilst still warm the filtrate concentrated by evaporation the residue recrystallised from a little methanol
Source ID: ord-6f3ffc5c3dae437286a22103a3ef822fConditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: A mixture of 23.0 g of 2,6-dihydroxybenzamide, 20.7 g of potassium carbonate and 28.2 g of 1,2-dibromoethane is refluxed, whilst stirring, for 2-3 hours in 300 ml of acetonitrile. The reaction mixture is filtered whilst still warm, the filtrate concentrated by evaporation and the residue recrystallised from a little methanol. 6-(2-Bromoethoxy)salicylamide having a melting point of 120°-121° is obtained. is refluxed The reaction mixture is filtered whilst still warm the filtrate concentrated by evaporation the residue recrystallised from a little methanol
Source ID: ord-47163b8fb6ae49a9b4394f743130485cConditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: A mixture of 23.0 g of 2,6-dihydroxybenzamide, 20.7 g of potassium carbonate and 28.2 g of 1,2-dibromoethane is refluxed, whilst stirring, for 2-3 hours in 300 ml of acetonitrile. The reaction mixture is filtered whilst still warm, the filtrate concentrated by evaporation and the residue recrystallised from a little methanol. 6-(2-Bromoethoxy)salicylamide having a melting point of 120°-121° is obtained. is refluxed The reaction mixture is filtered whilst still warm the filtrate concentrated by evaporation the residue recrystallised from a little methanol
Source ID: ord-47163b8fb6ae49a9b4394f743130485cConditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: A mixture of 23.0 g of 2,6-dihydroxybenzamide, 20.7 g of potassium carbonate and 28.2 g of 1,2-dibromoethane is refluxed, whilst stirring, for 2-3 hours in 300 ml of acetonitrile. The reaction mixture is filtered whilst still warm, the filtrate concentrated by evaporation and the residue recrystallised from a little methanol. 6-(2-Bromoethoxy)salicylamide having a melting point of 120°-121° is obtained. is refluxed The reaction mixture is filtered whilst still warm the filtrate concentrated by evaporation the residue recrystallised from a little methanol
Source ID: ord-2158019772d240b48c99ecea1fc7c2f3Conditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-96793f9fcc584dfda0813e03b1c3d606Conditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-77dca147f7b040fa94903350b02c0755Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: A mixture of 23.0 g of 2,6-dihydroxybenzamide, 20.7 g of potassium carbonate and 28.2 g of 1,2-dibromoethane is refluxed, whilst stirring, for 2-3 hours in 300 ml of acetonitrile. The reaction mixture is filtered whilst still warm, the filtrate concentrated by evaporation and the residue recrystallised from a little methanol. 6-(2-Bromoethoxy)salicylamide having a melting point of 120°-121° is obtained. is refluxed The reaction mixture is filtered whilst still warm the filtrate concentrated by evaporation the residue recrystallised from a little methanol
Source ID: ord-2158019772d240b48c99ecea1fc7c2f3Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: A mixture of 23.0 g of 2,6-dihydroxybenzamide, 20.7 g of potassium carbonate and 28.2 g of 1,2-dibromoethane in 300 ml of acetonitrile is stirred under reflux for 2-3 hours. The reaction mixture is filtered whilst still warm, the filtrate is evaporated and the residue is recrystallised from a little methanol. 6-(2-Bromoethoxy)salicylamide with a melting point of 120°-121° is obtained. under reflux for 2-3 hours The reaction mixture is filtered whilst still warm the filtrate is evaporated the residue is recrystallised from a little methanol
Source ID: ord-49770e2ac2594147b3c911489fde6c82Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: A mixture of 23.0 g of 2,6-dihydroxybenzamide, 20.7 g of potassium carbonate and 28.2 g of 1,2-dibromoethane is refluxed, whilst stirring, for 2-3 hours in 300 ml of acetonitrile. The reaction mixture is filtered whilst still warm, the filtrate concentrated by evaporation and the residue recrystallised from a little methanol. 6-(2-Bromoethoxy)salicylamide having a melting point of 120°-121° is obtained. is refluxed The reaction mixture is filtered whilst still warm the filtrate concentrated by evaporation the residue recrystallised from a little methanol
Source ID: ord-2158019772d240b48c99ecea1fc7c2f3PubChem References
These sources are listed in the compound's public database record.
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