01
Reaction #1595746
Reaction scheme
No renderable structure data available
No renderable structure data available
No renderable structure data available
Related Literature (1)
openreactiondata ↗doi:10.6084/m9.figshare.5104873.v1; patent:US04066434
Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: a solution of 54 parts of diethyl carbamoylphosphonate and 36 parts of dimethyl formamide dimethyl acetal was refluxed in 1000 parts of anhydrous tetrahydrofuran for eight hours. The solvent was removed under reduced pressure to give 70 parts of diethyl 1-dimethylaminomethyleneaminocarbonylphosphonate, nD24 = 1.4970. The solvent was removed under reduced pressure
Source ID: ord-604c31e06614499ba55501a3884b2024