2,3,3-trimethylbutan-2-amine;hydrochloride

Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

Procedure: 6.7 g. (0.044 mole) 2,3,3-trimethyl-2-butylamine hydrochloride and 3.4 g. (0.84 mole) NaOH in 20 ml. water are added to a stirred slurry of 3.6 g. (0.02 mole) cyanuric chloride in 150 ml. water. The reaction mixture is heated at reflux for 21/2 hours, cooled and filtered to give the product, a white solid, m.p. 129°-131° C., 6.5 g. The reaction mixture is heated at reflux for 21/2 hours cooled filtered to give the product

Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

Procedure: 6.7 g. (0.044 mole) 2,3,3-trimethyl-2-butylamine hydrochloride and 3.4 g. (0.84 mole) NaOH in 20 ml. water are added to a stirred slurry of 3.6 g. (0.02 mole) cyanuric chloride in 150 ml. water. The reaction mixture is heated at reflux for 21/2 hours, cooled and filtered to give the product, a white solid, m.p. 129°-131° C., 6.5 g. The reaction mixture is heated at reflux for 21/2 hours cooled filtered to give the product