No renderable structure data available
ClP(C(C)(C)C)ClChemical Intermediate
Structures, identifiers and computed properties have been matched to the database record by CAS.
| Intermediates | tert-Butyldichlorophosphine |
|---|---|
| IUPAC Name | — |
| CAS Number | 25979-07-1 |
| Database ID | 117690 |
| Molecular Formula | — |
| Molecular Weight | — |
Product Information
tert-Butyldichlorophosphine (CAS 25979-07-1) product identity, structure identifiers and related reaction data for chemical intermediate research and sourcing review.
Potential Applications
For professional research and industrial use only
Database ID 117690
Safety Notice
For professional research and industrial use only. Review the supplier safety data sheet before handling.
Synthesis data
10 reactions · 10 references
Conditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-dfe90852d659416a8f727713b674905eConditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-dfe90852d659416a8f727713b674905eConditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-dfe90852d659416a8f727713b674905eConditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: The starting material is prepared as follows: A mixture of 24.7 g of isopropanol and 17.2 g of triethylamine in 35 ml of diethylether is added drop by drop to 30 g of t-butyldichlorophosphine in 100 ml diethylether. The temperature is kept between 5° to 10°. The solid is filtered off and the filtrate evaporated. The crude oil is purified by distillation to yield t-butylphosphonous acid-isopropylester as an oil, b.p. 82°/2 kPa, nD20 =1.4222. The starting material is prepared is kept between 5° to 10° The solid is filtered off the filtrate evaporated The crude oil is purified by distillation
Source ID: ord-14f5ef5751e9452c87bcfb46ef1579f8Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: A mixture of 24.7 g of isopropanol and 17.2 g of triethylamine in 35 ml of diethylether is added drop by drop to 30 g of t-butyldichlorophosphine in 100 ml diethylether. The temperature is kept between 5 to 10°. The solid is filtered off and the filtrate evaporated. The crude oil is purified by distillation to yield t-butylphosphonous acid-isopropylester as an oil, b.p. 82°/2 kPa, nD20 =1.4222. is kept between 5 to 10° The solid is filtered off the filtrate evaporated The crude oil is purified by distillation
Source ID: ord-a5847f3abda447e5b46cb365a4283026Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: A mixture of 24.7 g of isopropanol and 17.2 g of triethylamine in 35 ml of diethylether is added drop by drop to 30 g of t-butyldichlorophosphine in 100 ml diethylether. The temperature is kept between 5 to 10°. The solid is filtered off and the filtrate evaporated. The crude oil is purified by distillation to yield t-butylphosphonous acid-isopropylester as an oil, b.p. 82°/2 kPa, n20D =1.4222. is kept between 5 to 10° The solid is filtered off the filtrate evaporated The crude oil is purified by distillation
Source ID: ord-6c99cdc2f205492e8f649a15c0dd75eaConditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: The starting material is prepared as follows: A mixture of 24.7 g of isopropanol and 17.2 g of triethylamine in 35 ml of diethylether is added drop by drop to 30 g of t-butyldichlorophosphine in 100 ml diethylether. The temperature is kept between 5° to 10°. The solid is filtered off and the filtrate evaporated. The crude oil is purified by distillation to yield t-butylphosphonous acid-isopropylester as an oil, b.p. 82°/2 kPa, nD20 =1.4222. The starting material is prepared is kept between 5° to 10° The solid is filtered off the filtrate evaporated The crude oil is purified by distillation
Source ID: ord-1f0425ff4479409aab7685f50a7506d0Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: A mixture of 24.7 g of isopropanol and 17.2 g of triethylamine in 35 ml of diethylether is added drop by drop to 30 g of t-butyldichlorophosphine in 100 ml diethylether. The temperature is kept between 5° to 10°. The solid is filtered off and the filtrate evaporated. The crude oil is purified by distillation to yield t-butylphosphonous acid-isopropylester as an oil, b.p. 82°/2 kPa, nD20 =1.4222. is kept between 5° to 10° The solid is filtered off the filtrate evaporated The crude oil is purified by distillation
Source ID: ord-82020e80d86b40eebaa8552b784e9530Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: The starting material is prepared as follows: A mixture of 24.7 g of isopropanol and 17.2 g of triethylamine in 35 ml of diethylether is added drop by drop to 30 g of t-butyldichlorophosphine in 100 ml diethylether. The temperature is kept between 5° to 10°. The solid is filtered off and the filtrate evaporated. The crude oil is purified by distillation to yield t-butylphosphonous acid-isopropylester as an oil, b.p. 82°/2 kPa, nD20 =1.4222. The starting material is prepared is kept between 5° to 10° The solid is filtered off the filtrate evaporated The crude oil is purified by distillation
Source ID: ord-14f5ef5751e9452c87bcfb46ef1579f8Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: A mixture of 24.7 g of isopropanol and 17.2 g of triethylamine in 35 ml of diethylether is added drop by drop to 30 g of t-butyldichlorophosphine in 100 ml diethylether. The temperature is kept between 5 to 10°. The solid is filtered off and the filtrate evaporated. The crude oil is purified by distillation to yield t-butylphosphonous acid-isopropylester as an oil, b.p. 82°/2 kPa, nD20 =1.4222. is kept between 5 to 10° The solid is filtered off the filtrate evaporated The crude oil is purified by distillation
Source ID: ord-a5847f3abda447e5b46cb365a4283026PubChem References
These sources are listed in the compound's public database record.
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