No renderable structure data available
CNC1CCC(CC1)OChemical Intermediate
Structures, identifiers and computed properties have been matched to the database record by CAS.
| Intermediates | 4-(methylamino)cyclohexan-1-ol |
|---|---|
| IUPAC Name | — |
| CAS Number | 22348-44-3 |
| Database ID | 11571804 |
| Molecular Formula | — |
| Molecular Weight | — |
Product Information
4-(methylamino)cyclohexan-1-ol (CAS 22348-44-3) product identity, structure identifiers and related reaction data for chemical intermediate research and sourcing review.
Potential Applications
For professional research and industrial use only
Database ID 11571804
Safety Notice
For professional research and industrial use only. Review the supplier safety data sheet before handling.
Synthesis data
12 reactions · 12 references
Conditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-dd9798038e6e477d838f388435326290Conditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-4b8fa99d7ebd4643ad16360ff0c8923aConditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-f88aa8030b0f4a1b990bc355404d8f45Conditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-2acf0bd861114d3a866b18c547518e32Conditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-0353c4dbeee049fc8c3d52e30a20947cConditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: Following procedures similar to those described in Example 260 there was obtained from 64.6 g. of 4-methylaminocyclohexanol, on reaction with 87.2 g. of 4-fluorobenzoyl chloride, 100.6 g. of 4-(N-methyl-4-fluorobenzamido)-cyclohexanol, m.p. 120°-130° C., 25.1 g. of which were oxidized to give 22.3 g. of 4-(N-methyl-4-fluorobenzamido)-cyclohexanone, m.p. 132°-136° C. was obtained from 64.6 g to give 22.3 g
Source ID: ord-3cabd50f6d864779bba5b0562a0691d4Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: Following procedures similar to those described in Example 260 there was obtained from 64.6 g. of 4-methylaminocyclohexanol, on reaction with 87.2 g. of 4-fluorobenzoyl chloride, 100.6 g. of 4-(N-methyl-4-fluorobenzamido)-cyclohexanol, m.p. 120°-130° C., 25.1 g. of which were oxidized to give 22.3 g. of 4-(N-methyl-4 -fluorobenzamido)-cyclohexanone, m.p. 132°-136° C. was obtained from 64.6 g to give 22.3 g
Source ID: ord-cbc90800ea664cefaf90a5ffd04606cdConditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: Following procedures similar to those described in Example 260 there was obtained from 64.6 g. of 4-methylaminocyclohexanol, on reaction with 87.2 g. of 4-fluorobenzoyl chloride, 100.6 g. of 4-(N-methyl-4-fluorobenzamido)-cyclohexanol, m.p. 120°-130° C., 25.1 g. of which were oxidized to give 22.3 g. of 4-(N-methyl-4 -fluorobenzamido)-cyclohexanone, m.p. 132°-136° C. was obtained from 64.6 g to give 22.3 g
Source ID: ord-cbc90800ea664cefaf90a5ffd04606cdConditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: Following procedures similar to those described in Example 260 there was obtained from 64.6 g. of 4-methylaminocyclohexanol, on reaction with 87.2 g. of 4-fluorobenzoyl chloride, 100.6 g. of 4-(N-methyl-4-fluorobenzamido)-cyclohexanol, m.p. 120°-130° C., 25.1 g. of which were oxidized to give 22.3 g. of 4-(N-methyl-4-fluorobenzamido)-cyclohexanone, m.p. 132°-136° C. was obtained from 64.6 g to give 22.3 g
Source ID: ord-3cabd50f6d864779bba5b0562a0691d4Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: Following procedures similar to those described in Example 260 there was obtained from 64.6 g. of 4-methylaminocyclohexanol, on reaction with 87.2 g. of 4-fluorobenzoyl chloride, 100.6 g. of 4-(N-methyl-4-fluorobenzamido)-cyclohexanol, m.p. 120°-130° C., 25.1 g. of which were oxidized to give 22.3 g. of 4-(N-methyl-4-fluorobenzamido)-cyclohexanone, m.p. 132°-136° C. was obtained from 64.6 g to give 22.3 g
Source ID: ord-3cabd50f6d864779bba5b0562a0691d4Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: Following procedures similar to those described in Example 260 there was obtained from 64.6 g. of 4-methylaminocyclohexanol, on reaction with 87.2 g. of 4-fluorobenzoyl chloride, 100.6 g. of 4-(N-methyl-4-fluorobenzamido)-cyclohexanol, m.p. 120°-130° C., 25.1 g. of which were oxidized to give 22.3 g. of 4-(N-methyl-4-fluorobenzamido)-cyclohexanone, m.p. 132°-136° C. was obtained from 64.6 g to give 22.3 g
Source ID: ord-c57a1b9fefa64cf0a6532bc89c724ec8Conditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-dd9798038e6e477d838f388435326290PubChem References
These sources are listed in the compound's public database record.
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