2-isothiocyanatopentane

Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

Procedure: The title compound was prepared from 2-amino-4,5-dichlorobenzenesulfonamide and 2-pentyl isothiocyanate by a method analogous to the one described in Example 4; m.p. 217-220° C. (ethyl acetate); 1H-NMR (DMSO-d6): δ 0.90 (t, 3H, CH3), 1.14 (d, 3H, CH3), 1.20-1.55 (m, 4H, CH2CH2), 3.83 (m, 1H, NHCH), 7.33 (br., 1H, NH), 7.49 (br.s, 1H, ArH), 7.89 (s, 1H, ArH), 10.48 (br.s, 1H, NH); MS: m/e 335/337/339 (M+).

Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

Procedure: The title compound was prepared from 2-amino-4,5-dichlorobenzenesulfonamide and 2-pentyl isothiocyanate by a method analogous to the one described in Example 4; m.p. 217-220° C. (ethyl acetate); 1H-NMR (DMSO-d6): δ 0.90 (t, 3H, CH3), 1.14 (d, 3H, CH3), 1.20-1.55 (m, 4H, CH2CH2), 3.83 (m, 1H, NHCH), 7.33 (br., 1H, NH), 7.49 (br.s, 1H, ArH), 7.89 (s, 1H, ArH), 10.48 (br.s, 1H, NH); MS: m/e 335/337/339 (M+).