3-isothiocyanatopentane

Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

Procedure: The title compound was prepared from 2-amino-4-chlorobenzenesulfonamide and 3-pentyl isothiocyanate by a method analogous to the one described in Example 4; m.p. 224-226° C. (ethyl acetate); 1H-NMR (DMSO-d6): δ 0.88 (t, 6H, 2×CH3), 1.33-1.66 (m, 4H, 2×CH2), 3.65 (m, 1H, CH), 7.1 (br.s, 1H, NH), 7.21-7.32 (m, 2H, ArH), 7.68 (d, 1H, ArH), 10.30 (br.s, 1H, NH); MS: m/e 301-303 (M+); (C12H16N3Cl1O2S1) calc. C, 47.76; H, 5.34; N, 13.92; found C, 47.74; H, 5.49; N, 13.93.

Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

Procedure: The title compound was prepared from 2-amino-4-chlorobenzenesulfonamide and 3-pentyl isothiocyanate by a method analogous to the one described in Example 4; m.p. 224-226° C. (ethyl acetate); 1H-NMR (DMSO-d6): δ 0.88 (t, 6H, 2×CH3), 1.33-1.66 (m, 4H, 2×CH2), 3.65 (m, 1H, CH), 7.1 (br.s, 1H, NH), 7.21-7.32 (m, 2H, ArH), 7.68 (d, 1H, ArH), 10.30 (br.s, 1H, NH); MS: m/e 301-303 (M+); (C12H16N3Cl1O2S1) calc. C, 47.76; H, 5.34; N, 13.92; found C, 47.74; H, 5.49; N, 13.93.

Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

Procedure: The title compound was prepared from 2-amino-4-chlorobenzenesulfonamide and 3-pentyl isothiocyanate by a method analogous to the one described in Example 4; m.p. 224-226° C. (ethyl acetate); 1H-NMR (DMSO-d6): δ 0.88 (t, 6H, 2×CH3), 1.33-1.66 (m, 4H, 2×CH2), 3.65 (m, 1H, CH), 7.1 (br.s, 1H, NH), 7.21-7.32 (m, 2H, ArH), 7.68 (d, 1H, ArH), 10.30 (br.s, 1H, NH); MS: m/e 301-303 (M+); (C12H16N3Cl1O2S1) calc. C, 47.76; H, 5.34; N, 13.92; found C, 47.74; H, 5.49; N, 13.93.