Reaction #3864789
Related Literature (1)
openreactiondata ↗doi:10.1039/C8SC04228D
Conditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-8463ddfc864f4395a7ce85481e0390ceNo renderable structure data available
CCCCCCCCCCCCC(CCC)OChemical Intermediate
Structures, identifiers and computed properties have been matched to the database record by CAS.
| Intermediates | 4-Hexadecanol |
|---|---|
| IUPAC Name | — |
| CAS Number | 19781-43-2 |
| Database ID | 34541 |
| Molecular Formula | — |
| Molecular Weight | — |
Product Information
4-Hexadecanol (CAS 19781-43-2) product identity, structure identifiers and related reaction data for chemical intermediate research and sourcing review.
Potential Applications
For professional research and industrial use only
Database ID 34541
Safety Notice
For professional research and industrial use only. Review the supplier safety data sheet before handling.
Synthesis data
11 reactions · 11 references
Conditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-8463ddfc864f4395a7ce85481e0390ceConditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: 2-hexadecanol; 3-hexadecanol; 4-hexadecanol;
Source ID: ord-9d8370b7c81a4b7dba31e82777a09a8dConditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: 4-Hexadecanol (12.29 g 0.051 mol) and p-Toluenesulfonyl chloride (12 g 0.063 mol) were dissolved Pyridine (100 ml) and stirred overnight at room temperature. Dichloromethane (400 ml) was added. Dichloromethane solution was then washed well with water, H2SO4 (3%), water, NaHCO3 (3%) and water, dried with anhydrous magnesium sulphate (10 g). After evaporation of the solvent 20 g of crude 4-Hexadecanesulfonyl chloride was obtained. Dichloromethane solution was then washed well with water, H2SO4 (3%), water, NaHCO3 (3%) and water dried with anhydrous magnesium sulphate (10 g) After evaporation of the solvent 20 g of crude 4-Hexadecanesulfonyl chloride was obtained
Source ID: ord-da09bdf779e241ce8305ad63b4c295a1Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: 4-Hexadecanol (12.29 g 0.051 mol) and p-Toluenesulfonyl chloride (12 g 0.063 mol) were dissolved Pyridine (100 ml) and stirred overnight at room temperature. Dichloromethane (400 ml) was added. Dichloromethane solution was then washed well with water, H2SO4 (3%), water, NaHCO3 (3%) and water, dried with anhydrous magnesium sulphate (10 g). After evaporation of the solvent 20 g of crude 4-Hexadecanesulfonyl chloride was obtained. Dichloromethane solution was then washed well with water, H2SO4 (3%), water, NaHCO3 (3%) and water dried with anhydrous magnesium sulphate (10 g) After evaporation of the solvent 20 g of crude 4-Hexadecanesulfonyl chloride was obtained
Source ID: ord-da09bdf779e241ce8305ad63b4c295a1Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: 2-hexadecanol; 3-hexadecanol; 4-hexadecanol;
Source ID: ord-9d8370b7c81a4b7dba31e82777a09a8dConditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: 2-hexadecanol; 3-hexadecanol; 4-hexadecanol;
Source ID: ord-9d8370b7c81a4b7dba31e82777a09a8dConditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: 4-Hexadecanol (12.29 g 0.051 mol) and p-Toluenesulfonyl chloride (12 g 0.063 mol) were dissolved Pyridine (100 ml) and stirred overnight at room temperature. Dichloromethane (400 ml) was added. Dichloromethane solution was then washed well with water, H2SO4 (3%), water, NaHCO3 (3%) and water, dried with anhydrous magnesium sulphate (10 g). After evaporation of the solvent 20 g of crude 4-Hexadecanesulfonyl chloride was obtained. Dichloromethane solution was then washed well with water, H2SO4 (3%), water, NaHCO3 (3%) and water dried with anhydrous magnesium sulphate (10 g) After evaporation of the solvent 20 g of crude 4-Hexadecanesulfonyl chloride was obtained
Source ID: ord-afa931a1bdb94d4aa05493a6545c8bb6Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: 4-Hexadecanol (12.29 g 0.051 mol) and p-Toluenesulfonyl chloride (12 g 0.063 mol) were dissolved Pyridine (100 ml) and stirred overnight at room temperature. Dichloromethane (400 ml) was added. Dichloromethane solution was then washed well with water, H2SO4 (3%), water, NaHCO3 (3%) and water, dried with anhydrous magnesium sulphate (10 g). After evaporation of the solvent 20 g of crude 4-Hexadecanesulfonyl chloride was obtained. Dichloromethane solution was then washed well with water, H2SO4 (3%), water, NaHCO3 (3%) and water dried with anhydrous magnesium sulphate (10 g) After evaporation of the solvent 20 g of crude 4-Hexadecanesulfonyl chloride was obtained
Source ID: ord-afa931a1bdb94d4aa05493a6545c8bb6Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: 2-hexadecanol; 3-hexadecanol; 4-hexadecanol;
Source ID: ord-a096f9eab5c845ed832489e7b0053100Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: 4-Hexadecanol (12.29 g 0.051 mol) and p-Toluenesulfonyl chloride (12 g 0.063 mol) were dissolved Pyridine (100 ml) and stirred overnight at room temperature. Dichloromethane (400 ml) was added. Dichloromethane solution was then washed well with water, H2SO4 (3%), water, NaHCO3 (3%) and water, dried with anhydrous magnesium sulphate (10 g). After evaporation of the solvent 20 g of crude 4-Hexadecanesulfonyl chloride was obtained. Dichloromethane solution was then washed well with water, H2SO4 (3%), water, NaHCO3 (3%) and water dried with anhydrous magnesium sulphate (10 g) After evaporation of the solvent 20 g of crude 4-Hexadecanesulfonyl chloride was obtained
Source ID: ord-da09bdf779e241ce8305ad63b4c295a1Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: 2-hexadecanol; 3-hexadecanol; 4-hexadecanol;
Source ID: ord-9d8370b7c81a4b7dba31e82777a09a8dPubChem References
These sources are listed in the compound's public database record.
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