01
Reaction #2214932
Reaction scheme
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No renderable structure data available
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Related Literature (1)
openreactiondata ↗doi:10.6084/m9.figshare.5104873.v1; patent:US04108885
Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: 14.25 g (0.075 mole) of N-(3-dimethylaminopropyl)-thiocarbamic acid-S-ethyl ester are dissolved in 250 ml of absolute ether. While stirring and cooling, dry HCl gas is introduced. After 1 hour the product is suction-filtered. One obtains 14.1 g (83.4% of the theory) of the Mp. 87°-93° C. After reprecipitation from isopropanol/ether one obtains a product of the Mp. 93°-94° C. cooling After 1 hour the product is suction-filtered One obtains 14.1 g (83.4% of the theory) of the Mp. 87°-93° C After reprecipitation from isopropanol/ether one obtains a product of the Mp. 93°-94° C.
Source ID: ord-ec01febba7ef4c04bc5991414eb69bb9