No renderable structure data available
CCCCCCC=CCC(=O)OChemical Intermediate
Structures, identifiers and computed properties have been matched to the database record by CAS.
| Intermediates | dec-3-enoic acid |
|---|---|
| IUPAC Name | — |
| CAS Number | 15469-77-9 |
| Database ID | 85855 |
| Molecular Formula | — |
| Molecular Weight | — |
Product Information
dec-3-enoic acid (CAS 15469-77-9) product identity, structure identifiers and related reaction data for chemical intermediate research and sourcing review.
Potential Applications
For professional research and industrial use only
Database ID 85855
Safety Notice
For professional research and industrial use only. Review the supplier safety data sheet before handling.
Synthesis data
12 reactions · 12 references
Conditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-dce148bb16c1426c80e37cc62bc85bfeConditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: To 4.5 g (27 mmol) of 3-decynoic acid from Example 30 dissolved in methanol in a Paar bottle is added 2 mg of nickel boride as catalyst. The bottle is flushed with hydrogen, sealed and pressurized with H2 at 2 pounds per square inch. The hydrogenation is allowed to proceed at room temperature for 2 hours. The methanol is stripped in vacuo and the residue is partitioned between ethyl acetate and in HCl. The ethyl acetate layer is separated, dried, (Na2SO4) and is stripped to afford an almost quantitative yield of 3-decenoic acid. The bottle is flushed with hydrogen sealed the residue is partitioned between ethyl acetate and in HCl The ethyl acetate layer is separated dried
Source ID: ord-f5e5f4fa30984fd8a42f29cd840a59abConditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: The 3-decenoic acid was converted to its corresponding acyl chloride (3-decenoyl chloride) by reaction with thionyl chloride.
Source ID: ord-11d25577ef6743df98772413c9ad14c5Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: The 3-decenoic acid was converted to its corresponding acyl chloride (3-decenoyl chloride) by reaction with thionyl chloride.
Source ID: ord-11d25577ef6743df98772413c9ad14c5Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: To 4.5 g (27 mmol) of 3-decynoic acid from Example 30 dissolved in methanol in a Paar bottle is added 2 mg of nickel boride as catalyst. The bottle is flushed with hydrogen, sealed and pressurized with H2 at 2 pounds per square inch. The hydrogenation is allowed to proceed at room temperature for 2 hours. The methanol is stripped in vacuo and the residue is partitioned between ethyl acetate and in HCl. The ethyl acetate layer is separated, dried, (Na2SO4) and is stripped to afford an almost quantitative yield of 3-decenoic acid. The bottle is flushed with hydrogen sealed the residue is partitioned between ethyl acetate and in HCl The ethyl acetate layer is separated dried
Source ID: ord-35cb007cd34a4d809d2f69580f544f96Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: The 3-decenoic acid was converted to its corresponding acyl chloride (3-decenoyl chloride) by reaction with thionyl chloride.
Source ID: ord-aef8a2a92dcb4699a8d05274419368c7Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: To 4.5 g (27 mmol) of 3-decynoic acid from Example 30 dissolved in methanol in a Paar bottle is added 2 mg of nickel boride as catalyst. The bottle is flushed with hydrogen, sealed and pressurized with H2 at 2 pounds per square inch. The hydrogenation is allowed to proceed at room temperature for 2 hours. The methanol is stripped in vacuo and the residue is partitioned between ethyl acetate and in HCl. The ethyl acetate layer is separated, dried, (Na2SO4) and is stripped to afford an almost quantitative yield of 3-decenoic acid. The bottle is flushed with hydrogen sealed the residue is partitioned between ethyl acetate and in HCl The ethyl acetate layer is separated dried
Source ID: ord-833a86c7a80647bdaffe07708abbad28Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: To 4.5 g (27 mmol) of 3-decynoic acid from Example 30 dissolved in methanol in a Paar bottle is added 2 mg of nickel boride as catalyst. The bottle is flushed with hydrogen, sealed and pressurized with H2 at 2 pounds per square inch. The hydrogenation is allowed to proceed at room temperature for 2 hours. The methanol is stripped in vacuo and the residue is partitioned between ethyl acetate and in HCl. The ethyl acetate layer is separated, dried, (Na2SO4) and is stripped to afford an almost quantitative yield of 3-decenoic acid. The bottle is flushed with hydrogen sealed the residue is partitioned between ethyl acetate and in HCl The ethyl acetate layer is separated dried
Source ID: ord-833a86c7a80647bdaffe07708abbad28Conditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-dce148bb16c1426c80e37cc62bc85bfeConditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: The 3-decenoic acid was converted to its corresponding acyl chloride (3-decenoyl chloride) by reaction with thionyl chloride.
Source ID: ord-96eca26405ab4aa4b46487f5a7d576abConditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: To 4.5g (27 mmol) of 3-decynoic acid from Example 30 dissolved in methanol in a Paar bottle is added 2mg of nickel boride as catalyst. The bottle is flushed with hydrogen, sealed and pressurized with H2 at 2 pounds per square inch. The hydrogenation is allowed to proceed at room temperature for 2 hours. The methanol is stripped in vacuo and the residue is partitioned between ethyl acetate and in HCl. The ethyl acetate layer is separated, dried, (Na2SO4) and is stripped to afford an almost quantitative yield of 3-decenoic acid. The bottle is flushed with hydrogen sealed the residue is partitioned between ethyl acetate and in HCl The ethyl acetate layer is separated dried
Source ID: ord-2885de98c4634b7dbdfdcc93533fb1baConditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: To 4.5 g (27 mmol) of 3-decynoic acid from Example 30 dissolved in methanol in a Paar bottle is added 2 mg of nickel boride as catalyst. The bottle is flushed with hydrogen, sealed and pressurized with H2 at 2 pounds per square inch. The hydrogenation is allowed to proceed at room temperature for 2 hours. The methanol is stripped in vacuo and the residue is partitioned between ethyl acetate and in HCl. The ethyl acetate layer is separated, dried, (Na2SO4) and is stripped to afford an almost quantitative yield of 3-decenoic acid. The bottle is flushed with hydrogen sealed the residue is partitioned between ethyl acetate and in HCl The ethyl acetate layer is separated dried
Source ID: ord-f5e5f4fa30984fd8a42f29cd840a59abPubChem References
These sources are listed in the compound's public database record.
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