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Reaction #1184739
Reaction scheme
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Related Literature (1)
openreactiondata ↗doi:10.6084/m9.figshare.5104873.v1; patent:US06080816
Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: Melt cyclohexanedimethanol in laboratory oven. When melted, take 294.7 g of cyclohexanedimethanol along with 0.11 g dibutyl tin dilaurate and place in a flask at about 35° C. Add 419.5 g of isocyanatopropyltrimethoxysilane over 75 minutes. Then hold for two hours. Cool and empty. at about 35° C Cool
Source ID: ord-49be91fd1619496aa33806af126dacb9