Reaction #3845494
Related Literature (1)
openreactiondata ↗doi:10.1039/C8SC04228D
Conditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-505ea6bfa76a44beaf6937e637e25a8fNo renderable structure data available
CCCCCCCCCCNCCOChemical Intermediate
Structures, identifiers and computed properties have been matched to the database record by CAS.
| Intermediates | 2-(decylamino)ethanol |
|---|---|
| IUPAC Name | — |
| CAS Number | 15196-28-8 |
| Database ID | 4060908 |
| Molecular Formula | — |
| Molecular Weight | — |
Product Information
2-(decylamino)ethanol (CAS 15196-28-8) product identity, structure identifiers and related reaction data for chemical intermediate research and sourcing review.
Potential Applications
For professional research and industrial use only
Database ID 4060908
Safety Notice
For professional research and industrial use only. Review the supplier safety data sheet before handling.
Synthesis data
12 reactions · 12 references
Conditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-505ea6bfa76a44beaf6937e637e25a8fConditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: A solution of aminoethanol (30.5 g, 500 mmol, 30.1 mL) and 1-bromodecane (27.65 g, 125 mmol, 26 mL) in ethanol was stirred at 65° C. for 4 hr. The solvent was removed under reduced pressure. The residue was diluted with EtOAc (800 mL) and the organic solution was washed with H2O (2×200 mL); saturated aqueous NaHCO3 (200 mL) and saturated brine (200 mL). The organic phase was dried over anhydrous Na2SO4, and concentrated under reduced pressure. The resulting crude product, 2-(decylamino)ethanol, was used without further purification. The solvent was removed under reduced pressure The residue was diluted with EtOAc (800 mL) the organic solution was washed with H2O (2×200 mL) The organic phase was dried over anhydrous Na2SO4 concentrated under reduced pressure The resulting crude product, 2-(decylamino)ethanol, was used without further purification
Source ID: ord-13053ecaab3f44b3bd5db3ca2a123c87Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: A solution of aminoethanol (30.5 g, 500 mmol, 30.1 mL) and 1-bromodecane (27.65 g, 125 mmol, 26 mL) in ethanol was stirred at 65° C. for 4 hr. The solvent was removed under reduced pressure. The residue was diluted with EtOAc (800 mL) and the organic solution was washed with H2O (2×200 mL); saturated aqueous NaHCO3 (200 mL) and saturated brine (200 mL). The organic phase was dried over anhydrous Na2SO4, and concentrated under reduced pressure. The resulting crude product, 2-(decylamino)ethanol, was used without further purification. The solvent was removed under reduced pressure The residue was diluted with EtOAc (800 mL) the organic solution was washed with H2O (2×200 mL) The organic phase was dried over anhydrous Na2SO4 concentrated under reduced pressure The resulting crude product, 2-(decylamino)ethanol, was used without further purification
Source ID: ord-13053ecaab3f44b3bd5db3ca2a123c87Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: A solution of aminoethanol (30.5 g, 500 mmol, 30.1 mL) and 1-bromodecane (27.65 g, 125 mmol, 26 mL) in ethanol was stirred at 65° C. for 4 hr. The solvent was removed under reduced pressure. The residue was diluted with EtOAc (800 mL) and the organic solution was washed with H2O (2×200 mL); saturated aqueous NaHCO3 (200 mL) and saturated brine (200 mL). The organic phase was dried over anhydrous Na2SO4, and concentrated under reduced pressure. The resulting crude product, 2-(decylamino)ethanol, was used without further purification. The solvent was removed under reduced pressure The residue was diluted with EtOAc (800 mL) the organic solution was washed with H2O (2×200 mL) The organic phase was dried over anhydrous Na2SO4 concentrated under reduced pressure The resulting crude product, 2-(decylamino)ethanol, was used without further purification
Source ID: ord-5c2d11e84f3143b581cce0ef62e83c36Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: A solution of aminoethanol (30.5 g, 500 mmol, 30.1 mL) and 1-bromodecane (27.65 g, 125 mmol, 26 mL) in ethanol was stirred at 65° C. for 4 hr. The solvent was removed under reduced pressure. The residue was diluted with EtOAc (800 mL) and the organic solution was washed with H2O (2×200 mL); saturated aqueous NaHCO3 (200 mL) and saturated brine (200 mL). The organic phase was dried over anhydrous Na2SO4, and concentrated under reduced pressure. The resulting crude product, 2-(decylamino)ethanol, was used without further purification. The solvent was removed under reduced pressure The residue was diluted with EtOAc (800 mL) the organic solution was washed with H2O (2×200 mL) The organic phase was dried over anhydrous Na2SO4 concentrated under reduced pressure The resulting crude product, 2-(decylamino)ethanol, was used without further purification
Source ID: ord-91ee54bef4f34732a4859ad6625da0c0Conditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-505ea6bfa76a44beaf6937e637e25a8fConditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: A solution of aminoethanol (30.5 g, 500 mmol, 30.1 mL) and 1-bromodecane (27.65 g, 125 mmol, 26 mL) in ethanol was stirred at 65° C. for 4 hr. The solvent was removed under reduced pressure. The residue was diluted with EtOAc (800 mL) and the organic solution was washed with 10 (2×200 mL); saturated aqueous NaHCO3 (200 mL) and saturated brine (200 mL). The organic phase was dried over anhydrous Na2SO4, and concentrated under reduced pressure. The resulting crude product, 2-(decylamino)ethanol, was used without further purification. The solvent was removed under reduced pressure The residue was diluted with EtOAc (800 mL) the organic solution was washed with 10 (2×200 mL) The organic phase was dried over anhydrous Na2SO4 concentrated under reduced pressure The resulting crude product, 2-(decylamino)ethanol, was used without further purification
Source ID: ord-ffacfc1d539a4eaf8aa41057464b33a0Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: A solution of aminoethanol (30.5 g, 500 mmol, 30.1 mL) and 1-bromodecane (27.65 g, 125 mmol, 26 mL) in ethanol was stirred at 65° C. for 4 hr. The solvent was removed under reduced pressure. The residue was diluted with EtOAc (800 mL) and the organic solution was washed with H2O (2×200 mL); saturated aqueous NaHCO3 (200 mL) and saturated brine (200 mL). The organic phase was dried over anhydrous Na2SO4, and concentrated under reduced pressure. The resulting crude product, 2-(decylamino)ethanol, was used without further purification. The solvent was removed under reduced pressure The residue was diluted with EtOAc (800 mL) the organic solution was washed with H2O (2×200 mL) The organic phase was dried over anhydrous Na2SO4 concentrated under reduced pressure The resulting crude product, 2-(decylamino)ethanol, was used without further purification
Source ID: ord-a9a00092b7824515ae10ed77ed9a9d9aConditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: A solution of aminoethanol (30.5 g, 500 mmol, 30.1 mL) and 1-bromodecane (27.65 g, 125 mmol, 26 mL) in ethanol was stirred at 65° C. for 4 hr. The solvent was removed under reduced pressure. The residue was diluted with EtOAc (800 mL) and the organic solution was washed with H2O (2×200 mL); saturated aqueous NaHCO3 (200 mL) and saturated brine (200 mL). The organic phase was dried over anhydrous Na2SO4, and concentrated under reduced pressure. The resulting crude product, 2-(decylamino)ethanol, was used without further purification. The solvent was removed under reduced pressure The residue was diluted with EtOAc (800 mL) the organic solution was washed with H2O (2×200 mL) The organic phase was dried over anhydrous Na2SO4 concentrated under reduced pressure The resulting crude product, 2-(decylamino)ethanol, was used without further purification
Source ID: ord-a9a00092b7824515ae10ed77ed9a9d9aConditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: A solution of aminoethanol (30.5 g, 500 mmol, 30.1 mL) and 1-bromodecane (27.65 g, 125 mmol, 26 mL) in ethanol was stirred at 65 ° C. for 4 hr. The solvent was removed under reduced pressure. The residue was diluted with EtOAc (800 mL) and the organic solution was washed with H2O (2×200 mL); saturated aqueous NaHCO3 (200 mL) and saturated brine (200 mL). The organic phase was dried over anhydrous Na2SO4, and concentrated under reduced pressure. The resulting crude product, 2-(decylamino)ethanol, was used without further purification. The solvent was removed under reduced pressure The residue was diluted with EtOAc (800 mL) the organic solution was washed with H2O (2×200 mL) The organic phase was dried over anhydrous Na2SO4 concentrated under reduced pressure The resulting crude product, 2-(decylamino)ethanol, was used without further purification
Source ID: ord-952fb4a214454a8db0b52f831480a11eConditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: A solution of aminoethanol (30.5 g, 500 mmol, 30.1 mL) and 1-bromodecane (27.65 g, 125 mmol, 26 mL) in ethanol was stirred at 65° C. for 4 hr. The solvent was removed under reduced pressure. The residue was diluted with EtOAc (800 mL) and the organic solution was washed with H2O (2×200 mL); saturated aqueous NaHCO3 (200 mL) and saturated brine (200 mL). The organic phase was dried over anhydrous Na2SO4, and concentrated under reduced pressure. The resulting crude product, 2-(decylamino)ethanol, was used without further purification. The solvent was removed under reduced pressure The residue was diluted with EtOAc (800 mL) the organic solution was washed with H2O (2×200 mL) The organic phase was dried over anhydrous Na2SO4 concentrated under reduced pressure The resulting crude product, 2-(decylamino)ethanol, was used without further purification
Source ID: ord-9ab85a7ae55644058a1b24be46c037c2Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: A solution of aminoethanol (30.5 g, 500 mmol, 30.1 mL) and 1-bromodecane (27.65 g, 125 mmol, 26 mL) in ethanol was stirred at 65° C. for 4 hr. The solvent was removed under reduced pressure. The residue was diluted with EtOAc (800 mL) and the organic solution was washed with H2O (2×200 mL); saturated aqueous NaHCO3 (200 mL) and saturated brine (200 mL). The organic phase was dried over anhydrous Na2SO4, and concentrated under reduced pressure. The resulting crude product, 2-(decylamino)ethanol, was used without further purification. The solvent was removed under reduced pressure The residue was diluted with EtOAc (800 mL) the organic solution was washed with H2O (2×200 mL) The organic phase was dried over anhydrous Na2SO4 concentrated under reduced pressure The resulting crude product, 2-(decylamino)ethanol, was used without further purification
Source ID: ord-4e9e7e7bf12a4aa9962579c5b14b83ebPubChem References
These sources are listed in the compound's public database record.
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