Reaction #3696569
Related Literature (1)
openreactiondata ↗doi:10.6084/m9.figshare.5104873.v1; patent:US04465783
Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: The mixture which was homogenised consisted of 119 g of titanium trichloride, 26 cm3 of butyl benzoate, 390 cm3 of toluene and 3 g of polystyrene ("Lustrex" HF 66). After operating the homogeniser at maximum power for 2.75 minutes, the contents of the flask had formed an immobile gel-like product and the temperature had risen to above 50° C. Homogenisation was terminated and 500 cm3 of toluene were added to assist in the transfer of the dispersed solid to a storage vessel. for 2.75 minutes the contents of the flask had formed an immobile gel-like product had risen to above 50° C Homogenisation was terminated 500 cm3 of toluene were added to assist in the transfer of the dispersed solid to a storage vessel
Source ID: ord-bf204b469be74984850856f66a1f4404