No renderable structure data available
CC(COC1=CC=CC=C1)OChemical Intermediate
Structures, identifiers and computed properties have been matched to the database record by CAS.
| Intermediates | 1-phenoxypropan-2-ol |
|---|---|
| IUPAC Name | — |
| CAS Number | 130879-97-9 |
| Database ID | 92839 |
| Molecular Formula | — |
| Molecular Weight | — |
Product Information
1-phenoxypropan-2-ol (CAS 130879-97-9) product identity, structure identifiers and related reaction data for chemical intermediate research and sourcing review.
Potential Applications
For professional research and industrial use only
Database ID 92839
Safety Notice
For professional research and industrial use only. Review the supplier safety data sheet before handling.
Synthesis data
12 reactions · 12 references
Conditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-79c49a7cbdca4bb1801f46fc104f46a1Conditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-96765150a4e840f6b3d24fb2b5733d65Conditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-2ec183714c754688aa2a6b139f9374e0Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: The present invention is directed to an antimicrobial composition and a method of using said composition, comprising an antimicrobially effective amount of DTEA and an amount of 1-butanol, cyclohexanol, hexyl alcohol, isobutanol, ethylene glycol phenyl ether, propylene glycol phenyl ether, or a mixture thereof effective to result in the antimicrobial composition having a freezing point of less than 0° C. at atmospheric pressure.
Source ID: ord-6671f0f928484bdda75d8a5c1b3147e4Conditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-79c49a7cbdca4bb1801f46fc104f46a1Conditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-79c49a7cbdca4bb1801f46fc104f46a1Conditions: temp:0.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: Phenoxy-2-propanone (3.4 mL, 25 mmol) was dissolved in ethanol (30 mL) and cooled to 0° C. Sodium borohydride (0.95 g; 25 mmol; 1 equiv.) was added. The mixture was stirred and allowed to warm to room temperature overnight. All of the starting material was gone according to tlc analysis, so the mixture was poured into water (30 mL) and ether (30 mL). The layers were separated and the aqueous layer was extracted with ether (2×20 mL). The organic layers were combined and concentrated. The resulting aqueous residue was poured into ether (25 mL). The organic layer was removed, dried (MgSO4), and concentrated to provide 1e (3.2 g; 85%). 1H nmr (300 MHz, CDCl3): 7.332-7.261 (3H, m); 6.995-6.904 (2H, m); 4.15-4.24 (1H, m); 3.972-3.768 (2H, m); 1.559 (1H, s); 1.290 (3H, d, J=6.38 Hz). IR (neat film, cm-1): 3350 (b, s); 2900 (s); 1590 (m). EIMS (m/e): 152 (M+). to warm to room temperature overnight The layers were separated the aqueous layer was extracted with ether (2×20 mL) concentrated The resulting aqueous residue was poured into ether (25 mL) The organic layer was removed dried (MgSO4) concentrated
Source ID: ord-a92c87fe015d4d3ba7d770b991676f8eConditions: temp:0.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: Phenoxy-2-propanone (3.4 mL, 25 mmol) was dissolved in ethanol (30 mL) and cooled to 0° C. Sodium borohydride (0.95 g; 25 mmol; 1 equiv.) was added. The mixture was stirred and allowed to warm to room temperature overnight. All of the starting material was gone according to tlc analysis, so the mixture was poured into water (30 mL) and ether (30 mL). The layers were separated and the aqueous layer was extracted with ether (2×20 mL). The organic layers were combined and concentrated. The resulting aqueous residue was poured into ether (25 mL). The organic layer was removed, dried (MgSO4), and concentrated to provide 1e (3.2 g; 85%). 1H nmr (300 MHz, CDCl3): 7.332-7.261 (3H, m); 6.995-6.904 (2H, m); 4.15-4.24 (1H, m); 3.972-3.768 (2H, m); 1.559 (1H, s); 1.290 (3H, d, J=6.38 Hz). IR (neat film, cm-1): 3350 (b, s); 2900 (s); 1590 (m). EIMS (m/e): 152 (M+). to warm to room temperature overnight The layers were separated the aqueous layer was extracted with ether (2×20 mL) concentrated The resulting aqueous residue was poured into ether (25 mL) The organic layer was removed dried (MgSO4) concentrated
Source ID: ord-a92c87fe015d4d3ba7d770b991676f8eConditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: The present invention is directed to an antimicrobial composition and a method of using said composition, comprising an antimicrobially effective amount of DTEA and an amount of 1-butanol, cyclohexanol, hexyl alcohol, isobutanol, ethylene glycol phenyl ether, propylene glycol phenyl ether, or a mixture thereof effective to result in the antimicrobial composition having a freezing point of less than 0° C. at atmospheric pressure.
Source ID: ord-6671f0f928484bdda75d8a5c1b3147e4Conditions: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
Procedure: The present invention is directed to an antimicrobial composition and a method of using said composition, comprising an antimicrobially effective amount of DTEA and an amount of 1-butanol, cyclohexanol, hexyl alcohol, isobutanol, ethylene glycol phenyl ether, propylene glycol phenyl ether, or a mixture thereof effective to result in the antimicrobial composition having a freezing point of less than 0° C. at atmospheric pressure.
Source ID: ord-6671f0f928484bdda75d8a5c1b3147e4Conditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-96765150a4e840f6b3d24fb2b5733d65Conditions: temp:0.00; pressure:0.00; stir:
Source ID: ord-2ec183714c754688aa2a6b139f9374e0PubChem References
These sources are listed in the compound's public database record.
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