4-bromo-2-fluorobenzonitrile

Conditions: temp:0.00; pressure:0.00; stir:

Conditions: temp:0.00; pressure:0.00; stir:

Conditions: temp:0.00; pressure:0.00; stir:

Conditions: temp:0.00; pressure:0.00; stir:

Conditions: temp:0.00; pressure:0.00; stir:

Conditions: temp:0.00; pressure:0.00; stir:

Conditions: temp:0.00; pressure:0.00; stir:

Conditions: temp:0.00; pressure:0.00; stir:

Conditions: temp:0.00; pressure:0.00; stir:

Conditions: temp:25.01; pressure:0.00; stir:

Conditions: temp:23.01; pressure:0.00; stir:

Procedure: Prior to irradiation, the reaction mixture was degassed by bubbling argon for 20 minutes diluted with saturated aqueous NaHCO3 extracted with Et2O (3 x 100 mL) washed with water and brine dried over MgSO4 concentrated in vacuo Fluka, 230-400 mesh, solvent system: 25% ethyl acetate/hexane

Conditions: temp:0.00; pressure:0.00; stir: